If you combine the counts from two of the seminal works on Crotalus [Gloyd (1940) and Klauber (1956)], you get the following:
Males: 19-32, mean: 25.7
Females: 16-26, mean 20.1
This appears to include a sizable overlap (19-26). However, these counts were made from specimens throughout the entire range of the species and include, I suspect, a number of clines and areas of localized geographic variation. If you consider a specific geographic area, the apparent overlap in counts should actually be less. For example: in 19 south Texas specimens for which I have subcaudal counts handy, there is no apparent overlap (although a larger sample would likely show some).
Males: 23-30, mean: 26.8 [n = 11]
Females: 18-22, mean: 20.9 [n = 8]
So, for south Texas one could apply the rule of thumb that a specimen with fewer than 23 subcaudals is probably female (probability increasing as the count goes lower), whereas one with 23 or more is probably a male (probability increasing as the count increases). Again, this is likely good only for south Texas. If you know where your specimen is from and you know the count ranges from that area, you can get very good results this way. Adult atrox from this area are pretty easily sexed visually, so I only use this strategy on neonates and small sub-adults.
Tom Lott